CRYSTAL-STRUCTURE OF BIS-N,N'-P-CHLORO-SALICYLIDENEAMINE-1,2-DIAMINOBENZENE

ELERMAN Y., ELMALI A., KABAK M., AYDIN M., PEDER M.

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, vol.24, no.9, pp.603-606, 1994 (SCI-Expanded, Scopus) identifier identifier

  • Publication Type: Article / Article
  • Volume: 24 Issue: 9
  • Publication Date: 1994
  • Doi Number: 10.1007/bf01671674
  • Journal Name: JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.603-606
  • Keywords: SCHIFF-BASES, MOLECULAR STRUCTURE
  • Ankara University Affiliated: No

Abstract

The crystal structure of the title compound, C20H14N2O2Cl2, has been determined by single crystal X-ray diffraction techniques. It crystallizes in the orthorhombic system with a = 7.532(3)Angstrom, b = 18.563(2)Angstrom, c = 25.089(3)Angstrom, space group Pbca, V = 3507.9(3)Angstrom(3), Z = 8, F(000) = 1584, D-x = 1.459 g cm(-3), M = 385.3 a.m.u., lambda(MoK alpha) = 0.7107 Angstrom, mu = 3.35 cm(-1), T = 297 degrees K, R = 0.086, R(w) = 0.049 for 2119 unique diffractometer data. The molecules are linked by van der Waals forces.